University :Mansoura University |
Faculty :Faculty of Science |
Department :Chemistry Department |
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| 1- 1- Course data :- |
| | Code: | 20318 | | Course title: | كيمياء تحليلية | | Year/Level: | ثالثة الكيمياء | | Program Title: | | | Specialization: | | | Teaching Hours: | Theoretical: | 3 | Tutorial: | 2 | Practical: | 6 |
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| 2- 2- Course aims :- |
| - Introduce the basic concepts of gravimetry, electrochemical analysis and chromatography.
- Study the different classes of thermal analysis.
- Learn the diverse techniques of electrochemical analysis.
- Introduce an idea about the electrodeposition and conductimetry.
- Study the chromatographic separation techniques and the various methods of extraction.
- Introduce an idea about the electrophoresis and the theory of HPLC.
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| 3- 3- Course Learning Outcomes :- |
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| 4- 4- Course contents :- |
| | No | Topics | Week No. |
|---|
| 1 | Gravimetry, thermogravimetry and volatilization: General principles -Preliminary treatment -Precipitation step –filtration and washing of the precipitate | | | 2 | • Drying or ignition of the precipitate | | | 3 | • Thermal analysis - volatilization or evolution methods | | | 4 | Electrochemical analysis: Introduction- Potentiometry- voltametry | | | 5 | • Polarography | | | 6 | • Electrodeposition coulometry- Conductimetry | | | 7 | Chromatographic separation techniques and methods of extraction: Phase equilibria and extractions chromatography | | | 8 | • Chromatographic systems- ion exchange- Paper chromatography | | | 9 | • Electrophoresis- High perfonnance liquid chromatography(Theory and instrumentation) | | | 10 | Practical: gravimetric analysis | |
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| 5- 5- Teaching and learning methods :- |
| | S | Method |
|---|
| Lectures using data show and board | | Problem classes and group tutorial | | Reports and discussion groups | | Laboratory work and assignment |
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| 6- 6- Teaching and learning methods of disables :- |
| - none
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| 7- 7- Student assessment :- |
| - Timing |
| | No | Method | Week No. |
|---|
| 1 | | 14 | | 2 | | 14 | | 3 | | 12 | | 4 | | 4, 8, 12 | | 5 | | 10 |
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| - Degree |
| | No | Method | Degree |
|---|
| 1 | Mid_term examination | 0 | | 2 | Final_term examination | 70 | | 3 | Oral examination | 10 | | 4 | Practical examination | 20 | | 5 | Semester work | 0 | | 6 | Other types of asessment | 0 | | Total | 100% |
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| 8- 8- List of books and references |
| | S | Reference | Type |
|---|
| 1 | Analytical chemistry | | | 2 | A short course in quantitative Analysis. Hobart H. Willard,1968. | | | 3 | Vogel's textbook of quantitative chemical analysis. A.I. Vogel, (1994 | | | 4 | www.elsevier.com | | | 5 | www.rsc.org.com | |
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| 9- 9- Matrix of knowledge and skills of the course |
| | S | Content | Study week |
|---|
| Gravimetry, thermogravimetry and volatilization: General principles -Preliminary treatment -Precipitation step –filtration and washing of the precipitate | | | • Drying or ignition of the precipitate | | | • Thermal analysis - volatilization or evolution methods | | | Electrochemical analysis: Introduction- Potentiometry- voltametry | | | • Polarography | | | • Electrodeposition coulometry- Conductimetry | | | Chromatographic separation techniques and methods of extraction: Phase equilibria and extractions chromatography | | | • Chromatographic systems- ion exchange- Paper chromatography | | | • Electrophoresis- High perfonnance liquid chromatography(Theory and instrumentation) | | | Practical: gravimetric analysis | |
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| Course Coordinator(s): - |
| - Ahmed Mohamed mabrok Elwakel
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| Head of department: - |
| Awad Ebrahim Ahmed Mohamed |
