University :Mansoura University |
Faculty :Faculty of Science |
Department :Chemistry Department |
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| 1- Course data :- |
| | Code: | 20417 | | Course title: | كيمياء تحليلية وتطبيقية | | Year/Level: | رابعة الكيمياء | | Program Title: | | | Specialization: | | | Teaching Hours: | Theoretical: | 4 | Tutorial: | 2 | Practical: | |
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| 2- Course aims :- |
| - Introduce the basic information of spectra of organic compounds.
- Introduce the principles of analysis of organic and inorganic compounds.
- Study the methods of analysis of ores and how to purify it.
- Study the physical and chemical properties of organic compounds by several techniques.
- Introduce the principles of X-ray, NMR, IR, and MS spectrometry.
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| 3- Course Learning Outcomes :- |
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| 4- Course contents :- |
| | No | Topics | Week |
|---|
| 1 | Spectrochemical analysis: Survey of spectrochemical methods | | | 2 | • Instrumentation-application | | | 3 | • Atomic spectroscopy atomic fluorescence and x-ray fluorescence spectroscopy applications | | | 4 | Applied spectroscopy: • IR spectroscopy-theory-units for hooks low-relation between wave number and the following factors: bond energy, bond length, electronegativity, s-character, ring sizes, conjugation, conformational analysis, mechanical coupling-vibration modes in polyatomic molecules, stretching vib, bending vib. | | | 5 | • UV and visible spectroscopy-theory-absorption law-chromophores and auxochrome-bathochromic effect - hypochromic effect hypochromic effect-Woodward rules of conjugated dienes, ?,?-unsaturated ketones, aromatic carbonyl compounds and polyenes-resonance in excited state, resonance in ground state, ketones and aldehydes-effect of pH-hydrogen bond, steric inhibition of conjugation-solvent correlation. | | | 6 | • NMR spectroscopy-theory-chemical shift-spin-spin coupling-integration - factors affecting chemical shift-inductive effect, anizotropic effect, Van der Wall effect, resonance, solvents, temperature, concentration, hydrogen bond | | | 7 | • MS spectrometry-theory and instruments-fragmentation rules (9 rules) | | | 8 | • Examples -structure elucidation using 4 spectra, IR, UV, NMR & MS. | | | 9 | Ore analysis and allied materials: Concentration of ores-sampling-choice of method | | | 10 | • Solution of the sample-preconcentration of traces | | | 11 | • Selective methods for the analysis of some elements-examples for complete analysis of some ores | | | 12 | • Processes, instruments and automated analysis | | | 13 | Applied inorganic chemistry: Raw materials- basic laws of chemical technology | | | 14 | • Basic types of processes- manufacture of inorganic chemical products | | | 15 | • Metal extraction - fuel cells. | |
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| 5- Teaching and learning methods :- |
| | S | Method |
|---|
| Lectures using board | | Home works | | reports and discussion groups |
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| 6- Teaching and learning methods of disables :- |
| No data found. |
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| 7- Student assessment :- |
| A. Timing |
| | No | Method | Week |
|---|
| 1 | | 14 | | 2 | | 14 | | 3 | | 4,8,12 | | 4 | | 10 |
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| B. Degree |
| | No | Method | Degree |
|---|
| 1 | Mid_term examination | 0 | | 2 | Final_term examination | 90 | | 3 | Oral examination | 10 | | 4 | Practical examination | 0 | | 5 | Semester work | 0 | | 6 | Other types of asessment | 0 | | Total | 100% |
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| 8- List of books and references |
| | S | Item | Type |
|---|
| 1 | Spectrochemical analysis | | | 2 | Applied of absorption spectroscopy | | | 3 | Applied inorganic chemistry | | | 4 | Ore analysis | | | 5 | Application of absorption spectroscopy of organic compounds, Jhon R. Dyer, 1987. | | | 6 | Analytical chemistry. An Introduction. Douglas A. Skoog, 1994. | | | 7 | Treatise on analytical chemistry. Analytical chemistry of inorganic and organic compounds. I. M. Kolthoff, 1978. | | | 8 | http://www.elsevier.com | |
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| 9- Matrix of knowledge and skills of the course |
| | S | Content | Study week |
|---|
| Spectrochemical analysis: Survey of spectrochemical methods | | | • Instrumentation-application | | | • Atomic spectroscopy atomic fluorescence and x-ray fluorescence spectroscopy applications | | | Applied spectroscopy: • IR spectroscopy-theory-units for hooks low-relation between wave number and the following factors: bond energy, bond length, electronegativity, s-character, ring sizes, conjugation, conformational analysis, mechanical coupling-vibration modes in polyatomic molecules, stretching vib, bending vib. | | | • UV and visible spectroscopy-theory-absorption law-chromophores and auxochrome-bathochromic effect - hypochromic effect hypochromic effect-Woodward rules of conjugated dienes, ?,?-unsaturated ketones, aromatic carbonyl compounds and polyenes-resonance in excited state, resonance in ground state, ketones and aldehydes-effect of pH-hydrogen bond, steric inhibition of conjugation-solvent correlation. | | | • NMR spectroscopy-theory-chemical shift-spin-spin coupling-integration - factors affecting chemical shift-inductive effect, anizotropic effect, Van der Wall effect, resonance, solvents, temperature, concentration, hydrogen bond | | | • MS spectrometry-theory and instruments-fragmentation rules (9 rules) | | | • Examples -structure elucidation using 4 spectra, IR, UV, NMR & MS. | | | Ore analysis and allied materials: Concentration of ores-sampling-choice of method | | | • Solution of the sample-preconcentration of traces | | | • Selective methods for the analysis of some elements-examples for complete analysis of some ores | | | • Processes, instruments and automated analysis | | | Applied inorganic chemistry: Raw materials- basic laws of chemical technology | | | • Basic types of processes- manufacture of inorganic chemical products | | | • Metal extraction - fuel cells. | |
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| Course Coordinator(s): - |
| - Shaban Elsaid Ghazy Ali
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| Head of department: - |
| Abd Elazeez Elsaid Elsaid Foda |
