الجامعة :جامعة المنصورة |
الكلية :كلية العلوم |
القسم :الكيمياء |
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| 1- بيانات المقرر :- |
| | الرمز الكودى: | 20417 | | اسم المقرر: | كيمياء تحليلية وتطبيقية | | الفرقة: | رابعة الكيمياء | | عنوان البرنامج: | | | التخصص: | | | عدد الساعات: | نظري: | 4 | فصل: | 2 | عملى: | |
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| 2- أهداف المقرر :- |
| - Introduce the basic information of spectra of organic compounds.
- Introduce the principles of analysis of organic and inorganic compounds.
- Study the methods of analysis of ores and how to purify it.
- Study the physical and chemical properties of organic compounds by several techniques.
- Introduce the principles of X-ray, NMR, IR, and MS spectrometry.
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| 3- نواتج التعلم المستهدفة للمقرر :- |
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| 4- محتويات المقرر :- |
| | م | الموضوع | الأسبوع |
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| 1 | Spectrochemical analysis: Survey of spectrochemical methods | | | 2 | • Instrumentation-application | | | 3 | • Atomic spectroscopy atomic fluorescence and x-ray fluorescence spectroscopy applications | | | 4 | Applied spectroscopy: • IR spectroscopy-theory-units for hooks low-relation between wave number and the following factors: bond energy, bond length, electronegativity, s-character, ring sizes, conjugation, conformational analysis, mechanical coupling-vibration modes in polyatomic molecules, stretching vib, bending vib. | | | 5 | • UV and visible spectroscopy-theory-absorption law-chromophores and auxochrome-bathochromic effect - hypochromic effect hypochromic effect-Woodward rules of conjugated dienes, ?,?-unsaturated ketones, aromatic carbonyl compounds and polyenes-resonance in excited state, resonance in ground state, ketones and aldehydes-effect of pH-hydrogen bond, steric inhibition of conjugation-solvent correlation. | | | 6 | • NMR spectroscopy-theory-chemical shift-spin-spin coupling-integration - factors affecting chemical shift-inductive effect, anizotropic effect, Van der Wall effect, resonance, solvents, temperature, concentration, hydrogen bond | | | 7 | • MS spectrometry-theory and instruments-fragmentation rules (9 rules) | | | 8 | • Examples -structure elucidation using 4 spectra, IR, UV, NMR & MS. | | | 9 | Ore analysis and allied materials: Concentration of ores-sampling-choice of method | | | 10 | • Solution of the sample-preconcentration of traces | | | 11 | • Selective methods for the analysis of some elements-examples for complete analysis of some ores | | | 12 | • Processes, instruments and automated analysis | | | 13 | Applied inorganic chemistry: Raw materials- basic laws of chemical technology | | | 14 | • Basic types of processes- manufacture of inorganic chemical products | | | 15 | • Metal extraction - fuel cells. | |
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| 5- أساليب التعليم والتعلم :- |
| | م | الاسلوب |
|---|
| Lectures using board | | Home works | | reports and discussion groups |
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| 6- أساليب التعليم والتعلم للطلاب ذوى القدرات المحدودة :- |
| لا توجد بيانات. |
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| 7- تقويم الطلاب :- |
| أ- التوقيت |
| | م | الطريقة | الأسبوع |
|---|
| 1 | | 14 | | 2 | | 14 | | 3 | | 4,8,12 | | 4 | | 10 |
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| ب- توزيع الدرجات |
| | م | الطريقة | الدرجة |
|---|
| 1 | امتحان نصف الترم | 0 | | 2 | امتحان آخر الترم | 90 | | 3 | الامتحان الشفوى | 10 | | 4 | الامتحان العملى | 0 | | 5 | أعمال الترم | 0 | | 6 | طرق أخرى للتقييم | 0 | | المجموع | 100% |
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| 8- قائمة الكتب الدراسية والمراجع |
| | م | العنصر | النوع |
|---|
| 1 | Spectrochemical analysis | | | 2 | Applied of absorption spectroscopy | | | 3 | Applied inorganic chemistry | | | 4 | Ore analysis | | | 5 | Application of absorption spectroscopy of organic compounds, Jhon R. Dyer, 1987. | | | 6 | Analytical chemistry. An Introduction. Douglas A. Skoog, 1994. | | | 7 | Treatise on analytical chemistry. Analytical chemistry of inorganic and organic compounds. I. M. Kolthoff, 1978. | | | 8 | http://www.elsevier.com | |
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| 9- مصفوفة المعارف والمهارات المستهدفة من المقرر الدراسي |
| | م | المحتوى | أسبوع الدراسة |
|---|
| Spectrochemical analysis: Survey of spectrochemical methods | | | • Instrumentation-application | | | • Atomic spectroscopy atomic fluorescence and x-ray fluorescence spectroscopy applications | | | Applied spectroscopy: • IR spectroscopy-theory-units for hooks low-relation between wave number and the following factors: bond energy, bond length, electronegativity, s-character, ring sizes, conjugation, conformational analysis, mechanical coupling-vibration modes in polyatomic molecules, stretching vib, bending vib. | | | • UV and visible spectroscopy-theory-absorption law-chromophores and auxochrome-bathochromic effect - hypochromic effect hypochromic effect-Woodward rules of conjugated dienes, ?,?-unsaturated ketones, aromatic carbonyl compounds and polyenes-resonance in excited state, resonance in ground state, ketones and aldehydes-effect of pH-hydrogen bond, steric inhibition of conjugation-solvent correlation. | | | • NMR spectroscopy-theory-chemical shift-spin-spin coupling-integration - factors affecting chemical shift-inductive effect, anizotropic effect, Van der Wall effect, resonance, solvents, temperature, concentration, hydrogen bond | | | • MS spectrometry-theory and instruments-fragmentation rules (9 rules) | | | • Examples -structure elucidation using 4 spectra, IR, UV, NMR & MS. | | | Ore analysis and allied materials: Concentration of ores-sampling-choice of method | | | • Solution of the sample-preconcentration of traces | | | • Selective methods for the analysis of some elements-examples for complete analysis of some ores | | | • Processes, instruments and automated analysis | | | Applied inorganic chemistry: Raw materials- basic laws of chemical technology | | | • Basic types of processes- manufacture of inorganic chemical products | | | • Metal extraction - fuel cells. | |
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| اساتذة المادة: - |
| - شعبان السيد غازى على
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| رئيس مجلس القسم العلمى: - |
| عبد العزيز السيد السيد فوده |
